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Ultra-Spherical Copper & Alloy Powders for AM | Optimized Ultrasonic Atomization Process

In the latest case study, 3DLab explores the optimization of ultrasonic atomization for pure copper and copper alloys, a critical advancement for additive manufacturing (AM) applications. R&D efforts focused on refining the atomization process to achieve high yields of perfectly spherical powders, ensuring superior performance in 3D printing, laser sintering, and other AM technologies.

Innovative Induction Melting & Ultrasonic Atomization

To transform copper scrap from production processes into high-quality powder, 3DLab utilized the proprietary induction melting system. This cutting-edge module leverages magnetic induction to melt the metal efficiently. By carefully controlling chamber pressure differentials, precisely dosed molten copper onto an ultrasonic atomization platform, where high-frequency vibrations generated uniform, spherical metal powders.

Process Optimization for Industrial Scalability

The research identifies key process optimizations that enhance atomization efficiency, yield, and powder quality. These advancements include:

  • Precision temperature & pressure control for consistent melt flow
  • Ultrasonic frequency tuning to minimize satellite particles
  • Real-time monitoring for improved powder sphericity and size distribution

These innovations ensure reliable, repeatable results, making ultrasonic atomization a viable solution for industrial-scale additive manufacturing.

Copper: Key Properties & Industrial Applications in Additive Manufacturing

Why Copper? Unmatched Conductivity, Durability & Machinability

Copper stands out as a critical material in advanced manufacturing due to its exceptional properties:

  • Thermal Conductivity (400 W/(m·K)) – Ideal for heat dissipation in high-performance systems.
  • Electrical Conductivity (58 × 10⁶ S/m) – Surpasses most metals, making it essential for electronics.
  • Corrosion Resistance – Maintains performance in harsh environments.
  • Excellent Machinability – Easily processed into complex components.

These characteristics make copper and its alloys indispensable across industries—particularly in additive manufacturing (AM), where high-purity powders are in demand.

Industrial Applications of Copper: From Aerospace to Electronics

1. Aerospace & Defense

Copper’s thermal management capabilities are vital for:

  • Heat exchangers
  • Avionic cooling systems
  • High-conductivity wiring

2. Automotive Industry

Electric vehicles (EVs) and traditional autos rely on copper for:

  • High-efficiency motors & inverters
  • Battery connectors & charging systems
  • Sensor and ECU components

3. Electronics & Semiconductor Manufacturing

As the backbone of modern circuitry, copper enables:

  • PCB (printed circuit board) traces
  • EMI shielding
  • High-speed data transmission lines

4. Construction & Energy

Copper’s durability and conductivity support:

  • Renewable energy systems (solar/wind)
  • Smart building infrastructure
  • Plumbing & HVAC applications

Overcoming Challenges in Copper Additive Manufacturing: Laser Reflectivity & Powder Quality

While copper’s exceptional thermal and electrical conductivity makes it ideal for additive manufacturing (AM), its material properties also introduce significant hurdles, particularly in laser-based processes like:

  • Selective Laser Melting (SLM)
  • Laser Powder Bed Fusion (LPBF)

1. High Laser Reflectivity: The Core Issue

Copper is the second most reflective metal after gold, bouncing back >90% of infrared (IR) laser energy (typical in most industrial lasers). This leads to:

  • Incomplete powder melting → Poor layer fusion
  • Low part density & increased porosity
  • Unstable melt pools & thermal inconsistencies

2. Solving the Laser Absorption Problem

Recent advancements suggest blue lasers (450–500 nm wavelength) as a breakthrough solution because:
✔ Shorter wavelengths = higher photon energy → Better copper absorption
✔ Reduced reflectivity → More efficient melting
✔ Improved part density & fewer defects

However, even with optimized lasers, powder quality remains critical.

The Role of High-Quality Copper Powder in AM Success

To maximize printability and performance, copper powders must meet strict criteria:

  • High sphericity → Ensures smooth powder flow and even packing
  • Low oxygen content → Prevents porosity and brittleness
  • Controlled particle size distribution → Optimizes laser interaction

Our ultrasonic atomization process (detailed in Part 1) addresses these needs by producing:

  • Perfectly spherical powders → Maximizing layer uniformity
  • Minimal satellites/defects → Reducing post-processing
  • Tailored particle sizes → Compatible with SLM/LPBF systems

By combining advanced laser technologies with ultrasonically atomized copper powders, manufacturers can overcome reflectivity challenges and unlock:

  • Dense, crack-free copper components
  • Higher conductivity in printed parts
  • Broader adoption in electronics, EVs, and aerospace


Research Methodology: From Raw Material to High-Quality Powder

Material Selection & Benchmarking

The study began with pure copper feedstock in multiple forms:

  • Sheets
  • Chips
  • Cylinders

Objective: Identify the optimal input form for:
✔ Fastest atomization speed
✔ Highest powder sphericity
✔ Lowest production cost

Ultrasonic Atomization System & Key Upgrades

3DLab employed a standard ultrasonic atomization setup but introduced critical refinements:

  • Enhanced melt flow control → Prevents oxide formation
  • Advanced crucible design → Improves thermal stability
  • Real-time process monitoring → Ensures repeatability

Key Challenges Overcome:

  • Minimizing oxygen pickup (oxide formation)
  • Eliminating crucible erosion
  • Achieving batch-to-batch consistency

Results: High-Yield, Sustainable Copper Powder Production

Performance Breakthroughs

After process optimization,  achieved:
✔  >90% yield of fine, spherical powder (ideal for AM)
✔  D50 particle size <45 µm with tight distribution
✔  Near-zero scrap due to closed-loop recycling

Efficiency & Sustainability Advantages

  • Faster cycle times → Higher throughput
  • Re-meltable scrap → 100% material utilization
  • Stable, repeatable process → Scalable for industry

Best Feedstock Form for AM Powders

Cylinders & plates proved optimal because:
✔ Higher melt volume per cycle → Lower energy cost
✔ Minimal surface oxidation → Cleaner atomization
✔ Easier handling → Improved automation potential

ATO LAB Plus advancements enable:

  • Cost-effective copper powder for LPBF/SLM
  • Sustainable production via scrap recycling
  • Reliable supply of high-sphericity powder

Next Steps: Scaling for industrial AM applications in electronics, EVs, and thermal management.

Expanding Ultrasonic Atomization to Copper Alloys

Building on our success with pure copper, we extended our ultrasonic atomization technology to two strategically important copper alloys:

1. Bronze (Cu-Sn Alloy)

  • Key Applications: Bearings, bushings, marine components
  • Atomization Advantages: Excellent oxidation resistance during processing

2. Incusil-ABA (Cu-Ag-In Alloy)

  • Key Applications: High-vacuum brazing, electronics packaging
  • Atomization Advantages: Maintains precise composition of volatile elements

Particle Size Distribution of atomized metal powders

Copper Bronze Incusil – ABA
Diameter [µm] Circularity Diameter [µm] Circularity Diameter [µm] Circularity
Average 50,74 0,97 50,74 0,93 50,57 0,93
Standard deviation 22,41 0,6 14,31 0,04 16,49 0,04
Max 111,02 1,0 119,45 1,0 100,55 1,0
Min 2,54 0,41 29,50 0,8 15,75 0,72

Key Findings:

  • Near-perfect sphericity (circularity >0.93) for all materials
  • Tight particle distribution (Span <1.2) ensuring consistent AM performance
  • High yield of usable powder (>89% in target size range)

Process Advantages for Alloy Systems

Our ultrasonic atomization technology demonstrates:
✔ Compositional integrity – No elemental segregation observed
✔ Low oxygen pickup – <200 ppm for all alloys
✔ Scalable production – Batch sizes up to 5 kg demonstrated

Industry Implications: Enabling New AM Applications

These results open doors for:

  • High-performance bronze components with optimized wear resistance
  • Precision Incusil-ABA parts for vacuum electronics
  • Multi-material AM systems using blended copper alloy powders

Conclusion: A Comprehensive Powder Production Solution

This study validates our ultrasonic atomization platform as:

  1. Versatile – Handles pure and alloyed copper systems
  2. Precise – Delivers consistent, spherical powders
  3. Scalable – Ready for industrial AM powder production

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